Prelab (semi-microscale experiment) 3
Prelab must include the mechanism of amide formation
Question 1 1
Question 2 (for amide synthesis only) 1
Question 4 1
Question 5 (draw rxn rate vs. pH-plot, see lecture) 2
SUBTOTAL PRE-LAB: 8 points
Recording of product weight 1
Recording of melting point 1
IR spectrum of product 2
Show product to TA 0
Initials in Lab Book after end of session 0
SUBTOTAL LAB: 4 points
Post-Lab Quest. 1 (amide synthesis only) 3
1-3 p. for absolute value of achieved yield
Post-Lab Quest. 2 (MP, IR, cf posted IR spectra) 3
Post-Lab Quest. 4 (assign) 1
Post-Lab Quest. 5 (see online H-NMR, see disc. in lecture) 1
SUBTOTAL POST-LAB: 8 points