Prelab (semi-microscale experiment) 3 Prelab must include the mechanism of amide formation Question 1 1 Question 2 (for amide synthesis only) 1 Question 4 1 Question 5 (draw rxn rate vs. pH-plot, see lecture) 2 SUBTOTAL PRE-LAB: 8 points Recording of product weight 1 Recording of melting point 1 IR spectrum of product 2 Show product to TA 0 Initials in Lab Book after end of session 0 SUBTOTAL LAB: 4 points Post-Lab Quest. 1 (amide synthesis only) 3 1-3 p. for absolute value of achieved yield Post-Lab Quest. 2 (MP, IR, cf posted IR spectra) 3 Post-Lab Quest. 4 (assign) 1 Post-Lab Quest. 5 (see online H-NMR, see disc. in lecture) 1 SUBTOTAL POST-LAB: 8 points